[CEPT] Solvothermal synthesis nano zinc oxide in  microwave reactor MSS2

Jacek Wojnarowicz ,  Tadeusz Chudoba ,  Witold Łojkowski ,  Sylwia Kuśnieruk ,  Elżbieta Pietrzykowska ,  Aleksandra Kędzierska ,  Agnieszka Opalińska 

Polish Academy of Sciences, Institute of High Pressure Physics (UNIPRESS), Sokolowska 29/37, Warszawa 01-142, Poland

Abstract
Laboratory Nanostructures for Photonics and Nanomedicine IWC PAN is an expert in the synthesis of doped nanoparticles with small size distribution using microwave technology solvothermal synthesis (MSS). MSS technology allows precise control parameters of nanoparticle synthesis such as reaction time, temperature and pressure. We obtain the zinc oxide particle size distribution in solvothermal synthesis which can be expressed as follows:
(CH3CO2) 2Zn  → ZnO

Synthesis of nano-zinc oxide doped with cobalt take place in solution of ethylene glycol during 12 minutes in microwave reactor MSS2. Specific surface doped ZnO is 10-50 m2/g and crystallites size are in a range from 20 to 150 nm.

Microwave, pressure chemical reactor MSS2 is used to carry out solvo- and hydrothermal microwavesynthesis, wherein is obtained nanopowders with specific particle size and morphology. Used  solutions in the reactor overtake a global level and allows to obtain ultrapure nanoparticles in the production and experimental scale. Developed high-pressure seals provide insert of substrates, running processes, released products in track made ​​from chemically inert materials.

 

Related papers
  1. Optical oxygen sensor for safe operation in hazardous areas
  2.   Optical oxygen sensor for safe operation  in hazardous areas
  3. Quo Vadis nanotechnology- for various stakeholders
  4. Opening of the Thursday Sessions of NanoPl 2014
  5. Microwave reactors for nanoparticle's synthesis
  6. Opening of Nano-Bio-Med session
  7. Bioactive GoHAP nanoparticles and their applications in medical implants technology
  8. Wykorzystanie metody NTA (Nanoparticle Tracking Analysis) w ocenie wielkości krążących mikrocząstek osocza i innych płynów fizjologicznych: pułapki i triki
  9. Advanced characterisation of nanomaterials according to ISO 17025 Norm

  10. Microwave solvothermal synthesis of resorbable nano-HAp with controlled grain size.
  11. Microwave Solvothermal Synthesis of High Quality Nanoparticles
  12. Microwave Solvothermal Synthesis of Nano Zinc Oxide Nanoparticles
  13. Microwave Solvothermal Technology (MSS) for nanoparticle synthesis
  14. Zaawansowana Charakteryzacja Nanocząstek
  15. [CEPT] Solvothermal synthesis and characterization of nanomaterials in the Laboratory of Nanostructures for Photonics and Nanomedicine, Center of Bio-Nanomaterials
  16. Scanning Electron Microscopy Investigations and Analysis of Nanostructures
  17. Polish Nanotechnology Platform - a discussion group at Linked-In
  18. Novel optical oxygen sensor for life and health protection made of nano-zirconia
  19. Nanometrology as a tool for nanotechnology problems solving
  20. Creating a Polish Nano-Bio-Technology and  Nano-Medicine Platform?
  21. MSS synthesis of highly biocompatible nano-HAP and coating of 3D poymer scaffolds
  22. Nanotechnologie w gospodarce województwa podlaskiego
  23. Characterization of nanomaterials according to EU recommendations, on the example of ZnO nanoparticles
  24. [CEPT] Nanohydroxyapatite-polylactide composites  for regenerative implants
  25. [CEPT] MSS synthesis of highly biocompatible nano-HAP with properties depending on the synthesis time.
  26. [CEPT] Studies of nanoparticles size distribution
  27. [CEPT] Studies of solubility of nanoparticles and stability of their suspension
  28. Iinvestigation of nanoparticles by DSC-TG methods accompanied by chemical analysis of emitted gas
  29. Green Technology and Pilot Unit for Manufacturing of Ultra Clean Concentrated Colloids of Nano Metals
  30. Presentation of the  Laboratory of Nanostructures for Photonics and Nanomedicine, Center of Bio-Nanomaterials, CePT
  31. ZnO nanoparticles effect on integrity of human endothelial cells
  32. Importance and trends in nanomedicine according  European Nanomedicine Platform survey
  33. Application of the Zeiss Ultra Plus scanning microscopy in bio-nanotechnology 
  34. Welcome address
  35. Otwarcie NanoInfoDay, Powitanie
  36. Characteristic of hydroxyapatite dense nanoceramic produced by The High Pressure Consolidation  
  37. Wpływ parametrów materiałowo-technicznych na właściwości optycznego czujnika tlenu na bazie nano-ZrO2
  38. Synteza nano-ZnO przy pomocy reaktora Mettler Toledo w Laboratorium Nanostruktur dla Fotoniki i Nanomedycyny CePT.
  39. Infrastruktura i specjalizacje nanotechnologii w Polsce na podstawie wyników ankiety NANOFORCE
  40. Solwotermalna synteza domieszkowanego nanotlenku cynku dla projektu NanoFATE. Otrzymywanie wodnych nanozawiesin domieszkowanego tlenku cynku.
  41. Nanotechnologia bezpieczna dla ludzi i przyjazna środowisku
  42. Badania rozkładu wielkości cząstek i potencjału zeta w Laboratorium Nanostruktur dla Fotoniki i Nanomedycyny CePT
  43. Badanie stabilności i rozpuszczalności zawiesin z nano ZnO i nano ZnO:Co otrzymanych w  Laboratorium Nanostrutur dla Fotoniki i Nanomedycyny CePT
  44. Badania nanoproszków przy pomocy technik DSC-TG/ QMS-FTIR w Laboratorium Nanostruktur dla Fotoniki i Nanomedycyny CePT
  45. Synthesis of highly biocompatible hydroxyapatite nanopowders
  46. Nanosafety - challenge of nowadays
  47. Influence of heat treatment on luminescence of ZrO+ Eu nanopowders
  48. Solvothermal synthesis of doped nano zinc oxide for the project NanoFATE.
  49. Podsumowanie
  50. Solwotermalna synteza domieszkowanego nano tlenku cynku dla projektu NanoFATE.
  51. Hydrothermal Synthesis of Zinc Oxide Nanopowders
  52. Optyczny sensor tlenu na bazie nanokrystalicznego ZrO2
  53. Solvothermal synthesis of nonstoichiometric hydroxyapatite nanoparticles
  54. Solvothermal synthesis of nonstoichiometric hydroxyapatite nanoparticles
  55. Procedury charakteryzacji nanoproszków
  56. Oferty nanoproszków - Laboratorium Nanostruktur, Instytut Wysokich Ciśnien PAN
  57. Nanofotonika dla małych i średnich przedsiębiorstw - mapy dorogowe i analizy SWOT  najważniejszych technologii.
  58. Otwarcie konferencji
  59. Polska  Platforma Nanotechnologii i zarys strategicznego programu "Nanotechnologia i wzrost inwestycji w B&R w Polsce"
  60. Nowe mikrofalowe reaktory do syntez nanocząstek - wybrane zagadnienia badawcze i przykłady zastosowań
  61. ZrO2:Tb nanopowders obtained by coprecipitation method
  62. ZnFe2O4/ZnO core-shell particles obtained by coprecipitation route
  63. Hydrothermal Synthesis of ZnAl2O4 Spinel
  64. Localization of rare-earth dopants in the lattice of nanocrystalline ZrO2 - EXAFS study
  65. Advanced nanoporous yttria-stabilized zirconia ceramics for luminescent oxygen sensors
  66. Excitation transfer in zirconia nanocrystals and ceramics
  67. Eu Luminescence in zirconia nanocrystals
  68. ZnO ceramic sintering and luminescence properties
  69. Oferta zaawansowanych materiałów w perspektywie 5 - 20 lat
  70. Strategia rozwoju badań nanoproszków
  71. Error bars in powder diffraction
  72. Synthesis of doped ZnO nanopowders in microwave hydrothermal reactors
  73. Characterization of nanopowders
  74. Synthesis of Al doped ZnO nanopowders and their enhanced luminescence
  75. Synthesis of nanopowders in supercritical water in a continuous flow reactor
  76. A summary of results obtained in Working Group 002 "Synthesis and Processing of Nanopowders"
  77. Summary of activities of Working Group D30/003 "Synthesis and Processing of Nanopowders"
  78. Doped zirconia nanopowders made in microwave – pressure reactor
  79. Combining microwave and pressure techniques for hydrothermal synthesis of ZnO and ZrO2 nanopowders doped with a range of metal ions
  80. Luminescence properties of zinc oxide nanopowders doped with Al ions obtained by the hydrothermal and vapour condensation methods.
  81. Surface chemistry of Pr-doped nanocrystalline zirconia
  82. Mechanical property of nano-TiO2 dispersed Al65Cu20Ti15 amorphous/nanocrystalline matrix bulk composite prepared by mechanical alloying and high pressure sintering
  83. Microwave technique applied on the hydrothermal synthesis and sintering of calcia stabilized zirconia nanoparticles
  84. Luminescence properties of cerium doped Y3Al5O12 nanopowders and nanoceramic
  85. Yttrium-Aluminum Garnet Synthesized in the Medium of Supercritical Fluids
  86. Advanced nanostructural zirconia ceramics for optical oxygen sensors
  87. Study of undoped and doped zirconia nanocrystals luminescence
  88. Doping of ZnO nanopowders with Mn, Ni and Cr In an ultrasound and microwave driver hydrothermal reaction
  89. Localization of rare-earth dopants in the lattice of nanocrystalline ZrO2 - EXAFS study
  90. Zirconia-based nanomaterials for oxygen sensor - generation, characterisation and optical properties
  91. Production of doped and non doped ceramics nanoparticles for optical applications
  92. Synthesis, sintering and properties of doped nanocrystalline powders of zirconia, zinc oxide and yttrium aluminum garnet (YAG)
  93. Characterization of nanocrystalline ZrO2 doped with Rare-Earth elements synthesized via High Pressure Hydrothermal Method
  94. Particle Size Distribution of ZrO2:Pr3+- Influences of pH, High Power Ultrasound, Surfactant and Dopant Quantity
  95. Time-Resolved Luminescence Characteristics of Doped YAG and YAP Nanopowders
  96. Cathodoluminescence of Al doped ZnO nanopowders
  97. Morphology of Al doped Zinc Oxide Obtained using Hydrothermal and Vapour Condensation Methods
  98. Luminescence and structural properties of rare-earth doped YAG nanoceramics
  99. Optimization of conditions of preparation of YAG nanopowders for sintering of translucent ceramics
  100. The influence of ZrO2 containing 10% Eu 3+ on the polyurethane hard domain structure of nano-composites with luminescence properties
  101. Growth and properties of ytterbium doped KY(WO4)2 nanocomposites
  102. Investigations on the utilization of nano zinc oxides synthesized by hydrothermal method in rubber compounds
  103. Doping of ZnO nanopowders with Mn and Cr in an ultrasound and microwave driven hydrothermal reaction
  104. Investigations of phase composition and grain size distribution in Pr doped ZrO2
  105. Nasze wyniki, zdania i sposoby ich realizacji
  106. Morphology of Al doped zinc oxide obtained by the vapour condensation method
  107. The comparison of the properties of YAG obtained by coprecipitation and SCR method
  108. Synthesis of nanopowders at elevated pressure and their characterisation - summary of work of the WG-002
  109. Accuracy of XRD size measurements of nanocrystals
  110. Morphology of Al-Doped Zinc Oxide Obtained by the Vapour Condensation Methods
  111. SWOT analysis of various reactors used for synthesis of nanopwoders in our Working Group
  112. Preliminary research on zirconia based optical oxygen sensor
  113. Preparation and electrical properties of the BaTiO3 nanoceramics
  114. Current trends in the development of metallic nanomaterials: results of a study carried out within the EC project Nanoroad SME
  115. Microstructural Evolution in Mechanical Alloying and Hot Pressing of Aluminium and 316 Stainless Steel Powder Blend
  116. Time-resolved luminescence of nanostructured ZnO
  117. Prediction of degree of localisation of misfit dislocation cores in intercrystalline interfaces based on interfacial adhesion
  118. Kinetic and thermodynamic factors leading to dissolution of cementite in pearlitic steel subjected to severe plastic deformation under pressure
  119. Yttria stabilized zirconia nanocrystals luminescence
  120. Application of XRD diffraction methods for determination of grain size distribution in nanoparticles
  121. Optical investigations of RE-doped YAG nanoceramics
  122. Electrical properties of nanocrystalline ZrO2 at high-pressure
  123. High-pressure Induced Structural Decomposition of RE-doped YAG Nanoceramics
  124. Synthesis of Al-doped ZnO nanomaterials with controlled luminescence properties
  125. Combination of ECAP and Hydrostatic Extrusion for ultra-fine grain (UFG) microstructure generation in 99.98% nickel.
  126. Mechanical properties and deformation behaviour of ultra-fine grained nickel.
  127. Grain Size and Grain Size Distribution of Nanocrystalline Pr-doped Zirconia Powders Obtained in High Pressure Microwave Reactor
  128. Influence of synthesis conditions on the particles size and the morphology of zinc oxide nanopowders
  129. Measuring the Grain Size Distribution of Pr-doped Zirconia Nanopowders obtained by Microwave Driven Hydrothermal Synthesis
  130. Excellent mechanical properties of UFG metals and alloys, subjected to combination of severe plastic deformation methods.
  131. An FT-IR Spectroscopic Investigation of Hydroxide Groups in Nano-Crystals of ZrO2.
  132. Development of microstructure and mechanical properties in nickel deformed by hydrostatic extrusion
  133. Structural and luminescence properties of yttrium-aluminum garnet (YAG) nanoceramics
  134. Biocompatibility of thin films based on hydrothermal synthesized HAp
  135. Hybrid HAp- maleic anhydride copolymer nanocomposites obtained by in situ functionalisation
  136. Fabrication and electrical properties of Eu3+:BaTiO3 nanoceramics for SOFC
  137. Luminescence of ZrO2 nanocrystals
  138. Molecular impurities in the luminescent ZnO nanocrystals
  139. X-Ray investigations of the natural and artificial White Etching Layer
  140. Diffusion and diffusion induced defects in GaN
  141. Excellent Mechanical Properties of Nickel Processed by High Pressure Techniques
  142. Microwave driven hydrothermal synthesis of iron oxide - the effect of process parameter on the properties of the nanopowders
  143. Relaxation processes in ZrO2 at high pressures
  144. Luminescence of ZrO2 and ZnO nanocrystals
  145. Zinc oxide nanopowders obtained by the microwave-hydrothermal route
  146. Microwave driven hydrothermal synthesis of Pr-doped zirconia nanopowders
  147. New hydroxyapatite based nanomaterials for potential use in medical fields
  148. Correlation between high-pressure ZrO2 electrical properties and crystallite size
  149. Precise determination of full Grain Size Distribution from diffraction peak profile as a result of kinematical theory of diffraction for polidispersive nanomaterials
  150. Pressure Effect on Grain Boundary Diffusion in Al Bicrystals
  151. Microstructure of Surface Layers of Raiways After Heavy Exploatation
  152. Application of High Pressure to Processing of Meat
  153. Normal Grain Growth in 2-d Strips of Polycrystalline Aluminium Under High Pressure
  154. Reaction Diffusion in Metallic Systems under High Pressure
  155. High Pressure Effect on Grain Boundary Wetting in Aluminium Bicrystals
  156. Pressure Effect on Interface Energy, Diffusion and Reactions
  157. Transformation of fractal microstructure of nanocrystalline SiC and diamond in high pressures - Small Angle Scattering Study
  158. Microwave-Hydrothermal Synthesis of Nanostructured Pr-Doped Zirconia Powders
  159. The Strain Induced Cementite Dissolution in Carbon Steels-Experimental Facts and Theoretical Approach
  160. Effect of SPD Grain Refinement and Peculiarity of Structure and Mechanical Properties of UFG Ni
  161. Luminescense of Nanosize ZrO2
  162. Structure, Morphology and Luminescence Properties of Pr-doped Nanocrystalline ZrO2 Obtained by Hydrothermal Method
  163. Nanostructure Formation on the Surface of Railway Tracks and Wheelsets
  164. Hydrothermal Synthesis of Zinc Oxide Nanopowders with Microwaves Applications
  165. Microwave Driven Hydrothermal Synthesis of Iron Oxide Nanopowders
  166. Indentation Technique for Determination if Mechanical Behavior of Nanomaterials (Bulk and Coatings)

Presentation: Poster at Nano and Advanced Materials Workshop and Fair, by Jacek Wojnarowicz
See On-line Journal of Nano and Advanced Materials Workshop and Fair

Submitted: 2013-09-10 09:49
Revised:   2013-09-10 10:22