Excellent mechanical properties of UFG metals and alloys, subjected to combination of severe plastic deformation methods.

Nikolay Krasilnikov 1,3Witold Łojkowski 2Ruslan Z. Valiev 1

1. Institute of Physics of Advanced Materials, Ufa State Aviation Technical University, K.Marks St.12, Ufa 450000, Russian Federation
2. Polish Academy of Sciences, High Pressure Research Center (UNIPRESS), Sokolowska 29/37, Warszawa 01-142, Poland
3. Ulyanovsk State University (UlGU), L.Tolstoy, 42, Ulyanovsk 432700, Russian Federation

Abstract

The Ni and Al-based alloy 2024 after different methods of severe plastic deformation (SPD) are investigated. The equal channel angular pressing (ECAP) and cold rolling nickel, subjected also to high-pressure torsion (HPT), is characterized of large strain degree, homogeneous structure with grain size 120 nm and shows at room temperature the record strength with ultimate tensile stress (UTS) (1270 MPa), but limited plasticity (6%). The combination of high strength and plasticity managed to be obtained using the annealing at 200C of Ni after ECAP and rolling. This treatment of Ni leads to UTS about 900 MPa and ductility 12%.
Using HPT under pressure 6 GPa has allowed to obtain nanostructured samples of Al-based alloy 2024 with grain size 70 nm and high-angle grain boundaries in result of torsion (5 turns) at room temperature. The nanostructured alloy at room temperature demonstrated record UTS above 1100 MPa, and superplastic behavior at temperature higher then 300С. The microhardness of nanostructured alloy after superplastic deformation was 1.5 GPa and was more than after standard treatment of coarse-grained state of alloy (1.2 GPa).
Opportunity of achievement in metals and alloys of combination high strength and good ductility opens perspectives of its application in industry, particularly, for mirco-systems and for details with complex geometry, obtained due to superplastic forming.

Related papers
  1. Hydrothermal Synthesis of ZnAl2O4 Spinel
  2. Localization of rare-earth dopants in the lattice of nanocrystalline ZrO2 - EXAFS study
  3. Advanced nanoporous yttria-stabilized zirconia ceramics for luminescent oxygen sensors
  4. Excitation transfer in zirconia nanocrystals and ceramics
  5. Eu Luminescence in zirconia nanocrystals
  6. ZnO ceramic sintering and luminescence properties
  7. Oferta zaawansowanych materiałów w perspektywie 5 - 20 lat
  8. Strategia rozwoju badań nanoproszków
  9. Error bars in powder diffraction
  10. Synthesis of doped ZnO nanopowders in microwave hydrothermal reactors
  11. Characterization of nanopowders
  12. Synthesis of Al doped ZnO nanopowders and their enhanced luminescence
  13. Synthesis of nanopowders in supercritical water in a continuous flow reactor
  14. A summary of results obtained in Working Group 002 "Synthesis and Processing of Nanopowders"
  15. Summary of activities of Working Group D30/003 "Synthesis and Processing of Nanopowders"
  16. Doped zirconia nanopowders made in microwave – pressure reactor
  17. Combining microwave and pressure techniques for hydrothermal synthesis of ZnO and ZrO2 nanopowders doped with a range of metal ions
  18. Luminescence properties of zinc oxide nanopowders doped with Al ions obtained by the hydrothermal and vapour condensation methods.
  19. Mechanical property of nano-TiO2 dispersed Al65Cu20Ti15 amorphous/nanocrystalline matrix bulk composite prepared by mechanical alloying and high pressure sintering
  20. Microwave technique applied on the hydrothermal synthesis and sintering of calcia stabilized zirconia nanoparticles
  21. Development and study of nanostructured titanium alloys with enhanced fatigue properties
  22. Luminescence properties of cerium doped Y3Al5O12 nanopowders and nanoceramic
  23. Yttrium-Aluminum Garnet Synthesized in the Medium of Supercritical Fluids
  24. Dissolution-precipitation of the secondary phase particles in copper-rich Cu-Cr alloys during high-pressure torsion
  25. Advanced nanostructural zirconia ceramics for optical oxygen sensors
  26. Study of undoped and doped zirconia nanocrystals luminescence
  27. Doping of ZnO nanopowders with Mn, Ni and Cr In an ultrasound and microwave driver hydrothermal reaction
  28. Localization of rare-earth dopants in the lattice of nanocrystalline ZrO2 - EXAFS study
  29. Zirconia-based nanomaterials for oxygen sensor - generation, characterisation and optical properties
  30. Production of doped and non doped ceramics nanoparticles for optical applications
  31. Synthesis, sintering and properties of doped nanocrystalline powders of zirconia, zinc oxide and yttrium aluminum garnet (YAG)
  32. Characterization of nanocrystalline ZrO2 doped with Rare-Earth elements synthesized via High Pressure Hydrothermal Method
  33. Particle Size Distribution of ZrO2:Pr3+- Influences of pH, High Power Ultrasound, Surfactant and Dopant Quantity
  34. Time-Resolved Luminescence Characteristics of Doped YAG and YAP Nanopowders
  35. Cathodoluminescence of Al doped ZnO nanopowders
  36. Morphology of Al doped Zinc Oxide Obtained using Hydrothermal and Vapour Condensation Methods
  37. Luminescence and structural properties of rare-earth doped YAG nanoceramics
  38. Optimization of conditions of preparation of YAG nanopowders for sintering of translucent ceramics
  39. The influence of ZrO2 containing 10% Eu 3+ on the polyurethane hard domain structure of nano-composites with luminescence properties
  40. Growth and properties of ytterbium doped KY(WO4)2 nanocomposites
  41. Investigations on the utilization of nano zinc oxides synthesized by hydrothermal method in rubber compounds
  42. Doping of ZnO nanopowders with Mn and Cr in an ultrasound and microwave driven hydrothermal reaction
  43. Investigations of phase composition and grain size distribution in Pr doped ZrO2
  44. Nasze wyniki, zdania i sposoby ich realizacji
  45. Morphology of Al doped zinc oxide obtained by the vapour condensation method
  46. The comparison of the properties of YAG obtained by coprecipitation and SCR method
  47. Synthesis of nanopowders at elevated pressure and their characterisation - summary of work of the WG-002
  48. Accuracy of XRD size measurements of nanocrystals
  49. Morphology of Al-Doped Zinc Oxide Obtained by the Vapour Condensation Methods
  50. SWOT analysis of various reactors used for synthesis of nanopwoders in our Working Group
  51. Preliminary research on zirconia based optical oxygen sensor
  52. Preparation and electrical properties of the BaTiO3 nanoceramics
  53. Current trends in the development of metallic nanomaterials: results of a study carried out within the EC project Nanoroad SME
  54. Microstructural Evolution in Mechanical Alloying and Hot Pressing of Aluminium and 316 Stainless Steel Powder Blend
  55. Time-resolved luminescence of nanostructured ZnO
  56. Prediction of degree of localisation of misfit dislocation cores in intercrystalline interfaces based on interfacial adhesion
  57. Kinetic and thermodynamic factors leading to dissolution of cementite in pearlitic steel subjected to severe plastic deformation under pressure
  58. Yttria stabilized zirconia nanocrystals luminescence
  59. Application of XRD diffraction methods for determination of grain size distribution in nanoparticles
  60. Optical investigations of RE-doped YAG nanoceramics
  61. Electrical properties of nanocrystalline ZrO2 at high-pressure
  62. High-pressure Induced Structural Decomposition of RE-doped YAG Nanoceramics
  63. Synthesis of Al-doped ZnO nanomaterials with controlled luminescence properties
  64. The New SPD Processing Routes to Fabricate Bulk Nanostructured Materials
  65. Combination of ECAP and Hydrostatic Extrusion for ultra-fine grain (UFG) microstructure generation in 99.98% nickel.
  66. Phase transformations in pearlitic steels induced by severe plastic deformation.
  67. Mechanical properties and deformation behaviour of ultra-fine grained nickel.
  68. Deformation-induced nanocrystallization in Al-rich metallic glasses
  69. X-RAY ANALYSIS OF HIGH PRESSURE TORSION INDUCED NANOSTRUCTURES IN TI AND NI
  70. STRENGTH OF COMMERCIAL ALUMINUM ALLOYS AFTER EQUAL CHANNEL ANGULAR PRESSING (ECAP) AND POST-ECAP PROCESSING
  71. Сombined SPD techniques for fabrication of nanostructured Ti rods for medical applications
  72. Grain Size and Grain Size Distribution of Nanocrystalline Pr-doped Zirconia Powders Obtained in High Pressure Microwave Reactor
  73. Influence of synthesis conditions on the particles size and the morphology of zinc oxide nanopowders
  74. Measuring the Grain Size Distribution of Pr-doped Zirconia Nanopowders obtained by Microwave Driven Hydrothermal Synthesis
  75. An FT-IR Spectroscopic Investigation of Hydroxide Groups in Nano-Crystals of ZrO2.
  76. Development of microstructure and mechanical properties in nickel deformed by hydrostatic extrusion
  77. Structural and luminescence properties of yttrium-aluminum garnet (YAG) nanoceramics
  78. Biocompatibility of thin films based on hydrothermal synthesized HAp
  79. Hybrid HAp- maleic anhydride copolymer nanocomposites obtained by in situ functionalisation
  80. Fabrication and electrical properties of Eu3+:BaTiO3 nanoceramics for SOFC
  81. Luminescence of ZrO2 nanocrystals
  82. Molecular impurities in the luminescent ZnO nanocrystals
  83. X-Ray investigations of the natural and artificial White Etching Layer
  84. Diffusion and diffusion induced defects in GaN
  85. Excellent Mechanical Properties of Nickel Processed by High Pressure Techniques
  86. Microwave driven hydrothermal synthesis of iron oxide - the effect of process parameter on the properties of the nanopowders
  87. Relaxation processes in ZrO2 at high pressures
  88. Luminescence of ZrO2 and ZnO nanocrystals
  89. Zinc oxide nanopowders obtained by the microwave-hydrothermal route
  90. Microwave driven hydrothermal synthesis of Pr-doped zirconia nanopowders
  91. New hydroxyapatite based nanomaterials for potential use in medical fields
  92. Recent progress in developing nanostructured SPD materials with unique properties
  93. Mechanical properties nanostructured iron obtained by different methods of Severe Plastic Deformation
  94. Correlation between high-pressure ZrO2 electrical properties and crystallite size
  95. TiNi-based shape memory alloys for medical application
  96. Precise determination of full Grain Size Distribution from diffraction peak profile as a result of kinematical theory of diffraction for polidispersive nanomaterials
  97. Pressure Effect on Grain Boundary Diffusion in Al Bicrystals
  98. Microstructure of Surface Layers of Raiways After Heavy Exploatation
  99. Normal Grain Growth in 2-d Strips of Polycrystalline Aluminium Under High Pressure
  100. Reaction Diffusion in Metallic Systems under High Pressure
  101. High Pressure Effect on Grain Boundary Wetting in Aluminium Bicrystals
  102. Nanostructured Materials from Severe Plastic Deformation under High Pressure
  103. Pressure Effect on Interface Energy, Diffusion and Reactions
  104. Microwave-Hydrothermal Synthesis of Nanostructured Pr-Doped Zirconia Powders
  105. The Strain Induced Cementite Dissolution in Carbon Steels-Experimental Facts and Theoretical Approach
  106. United Approach to the Description of Diffusion in Equilibrium and Nonequilibrium Grain Boundaries and its Application to Nanomaterials
  107. The Nanostructured Tini Shape-Memory Alloys: New Properties and Applications
  108. Effect of SPD Grain Refinement and Peculiarity of Structure and Mechanical Properties of UFG Ni
  109. Luminescense of Nanosize ZrO2
  110. Structure, Morphology and Luminescence Properties of Pr-doped Nanocrystalline ZrO2 Obtained by Hydrothermal Method
  111. Nanostructure Formation on the Surface of Railway Tracks and Wheelsets
  112. Hydrothermal Synthesis of Zinc Oxide Nanopowders with Microwaves Applications
  113. Microwave Driven Hydrothermal Synthesis of Iron Oxide Nanopowders
  114. Indentation Technique for Determination if Mechanical Behavior of Nanomaterials (Bulk and Coatings)

Presentation: oral at E-MRS Fall Meeting 2004, Symposium I, by Nikolay A. Krasilnikov
See On-line Journal of E-MRS Fall Meeting 2004

Submitted: 2004-06-17 11:49
Revised:   2004-06-17 11:51
Google
 
Web science24.com
© 1998-2008 pielaszek research, all rights reserved Powered by the Conference Engine