The using of high temperature X-ray diffraction for in situ investigation of processes in liquid metal – solid non metal material systems. The mix of corresponding powders is used as experimental sample. The method was tested for alumina - Ag-Cu-Ti system. The formation of titanium monoxide was observed at high temperature, these results confirms the generally accepted theory. Barium titanate - Cu-Ti and calcium fluoride - Cu-Ti systems were also studied.

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